Mirror Facets for VERITAS Telescopes
E. ROACHE1, R. IRVIN1, J. S. PERKINS1, K. HARRIS2, A. FALCONE3, J. FINLEY4 AND T. WEEKES1
Read the full paper, including figures and technical drawings, using the PDF viewer or download link to the left. Full text is transcribed below for accessibility.
Mirror Facets for VERITAS Telescopes
E. ROACHE1, R. IRVIN1, J. S. PERKINS1, K. HARRIS2, A. FALCONE3, J. FINLEY4 AND T. WEEKES1
Read the full paper, including figures and technical drawings, using the PDF viewer or download link to the right. Full text is transcribed below for accessibility.
30TH INTERNATIONAL COSMIC RAY CONFERENCE
ICRC’07
Mérida, México
Mirror Facets for the VERITAS Telescopes
E. ROACHE1, R. IRVIN1, J. S. PERKINS1, K. HARRIS2, A. FALCONE3, J. FINLEY4 AND T. WEEKES1
1 Smithsonian Astrophysical Observatory, 670 Mount Hopkins Road, Amado, AZ
2 EOS Technologies, 3160 E. Transcon Way, Tucson, AZ
3 Pennsylvania State University, 104 Davey Lab, University Park, PA
4 Purdue University, 525 Northwestern Avenue, Lafayette, IN
roache@egret.sao.arizona.edu
Abstract:
Each of the VERITAS telescopes has 345 glass facets. These were manufactured by D.O.T.I. (Round Rock, Texas), by slumping and grinding to get the desired optical figure. The facets were aluminized and anodized at the Whipple Observatory. The reflectivity, radius of curvature and spot size were measured. The design specifications for reflectivity (90% at 320 nm and ≥ 85% between 280 nm and 450 nm), radius of curvature (24 m ± 1%) and spot size (<10 mm at radius of curvature) were easily met. The aluminizing and anodizing process are described as well as the effects of exposure at the VERITAS site on the reflectivity.
Introduction
In early 2003 work began on the first of the four VERITAS telescopes at the Whipple Observatory. Displays and Optical Technologies Inc. (D.O.T.I.) of Round Rock, TX supplied the 1,470 VERITAS glass facets. To produce the best quality mirror facets as quickly as possible the gamma ray mirror coating facility was moved from Mt. Hopkins to the Observatory basecamp. With a new, cleaner, mirror lab, an upgraded vacuum pump and new glass from D.O.T.I., we were able to produce mirror coatings of a quality exceeding any on the 10 m telescope. Continuing the decision made in 1992 we no longer use a quartz overcoat. Our aluminum coatings are anodized and have a hard aluminum oxide surface. This anodized surface is much less prone to deterioration than the quartz treatment, is less costly to produce and can be washed as needed.
Glass
VERITAS mirrors are hexagonal facets which measure 60.96 ± 0.3 cm across the flat sides (width) with a radius of curvature (RoC) measuring 24 m ± 1%. The mirrors are slumped glass 11.5 ± 1.0 mm thick and aluminized on the front surface. The energy concentration of each mirror allows for more than 90% of the reflected light to fall within a 10 mm diameter circle located at the radius of curvature. An alignment of all mirrors on the telescope produces a point spread function of 0.06° (at 70° elevation, with a bias alignment), which is well within the pixel size of the camera.
To achieve a high quality aluminum coating, it is essential that the glass be thoroughly cleaned. The glass is washed with a phosphate-free mild detergent (Liquinox) to remove the surface dirt. This is followed by a rinsing with tap water and a final rinsing with distilled water. The glass is then dried in an upright position to help keep it clean. Prior to loading the glass into the aluminizing chamber, the glass is wiped with isopropyl alcohol (99% electronic grade). Once in the chamber, the glass is “dusted” with carbon dioxide snow, to remove any lint or dust present on the glass surface. A final microscopic cleaning using ionized argon is performed under vacuum just prior to the deposition of aluminum [1].
Figure 1 caption: Anodized and un-anodized mirror reflectivity versus wavelength. The un-anodized mirror has a relatively flat wavelength response compared to the anodized mirror. However, anodization greatly increases the lifetime of the mirror.
Aluminizing
Aluminizing is the process of evaporating aluminum onto the glass surface to create a mirror. The evaporation must be done under vacuum to ensure the purity of the coating, which is important for optical properties and strong adhesion [2]. The aluminizing chamber measures roughly one cubic meter internally and easily accommodates a single facet. The glass is suspended from the top of the chamber, facing downwards. About 75 cm below the glass is a 7.5 cm long tungsten filament supporting 30–40 aluminum staples. These staples consist of 99.999% pure, 1 mm diameter aluminum cut to a length of approximately 4 cm. The pressure inside the chamber is reduced first by a 150 cfm Stokes fore pump and then by a Varian Turbo Molecular pump. The final vacuum needed for deposition is in the mid 10⁻⁵ Torr range. This is the optimal vacuum to ensure both time and quality requirements are met. The thickness of the coating is measured using a 5 MHz quartz crystal oscillator mounted inside the chamber adjacent to the glass facet [3]. The average aluminum coating is 180 nm thick, deposited at a rate of between 3 and 8 nm per second. A minimum allowed coating of 135 nm was established to ensure a uniform reflectivity across the surface of the mirror. The entire coating process (per mirror) takes about one hour.
Figure 2 caption: VERITAS telescope mirror reflectivity versus wavelength broken down by telescope. The design specified reflectivities of 90% at 320 nm and ≥ 85% between 280 nm and 450 nm.
Anodization
Traditional telescope mirrors are coated with pure aluminum. As aluminum is easily weathered, most telescopes are protected by a dome. Unfortunately, this is not feasible for air Cherenkov telescopes. Previously, a protective quartz overcoating was used on the 10 m telescope. However, pitting in the overcoating led to rapid deterioration of the aluminum reflectivity, and this method was abandoned in 1992 in favor of anodization [3].
Anodization is a process in which the top layer of the pure aluminum coating is converted into a harder and more durable layer of aluminum oxide. This is accomplished by passing a current of electricity through the aluminum coating while it is submerged in an electrolyte solution. The electrical circuit consists of the cathode (mirror surface), electrolyte solution and the anode (aluminum coil). The cathode makes contact with the aluminum coating at the three mounting holes to produce an even current distribution and minimize the un-anodized surface area. The contact material is 000-steel wool which is kept dry by compressing rubber o-rings against the aluminum coating. The electrolyte is a weak acidic solution (pH 5.5) containing ammonium hydroxide, tartaric acid, distilled water and ethylene glycol. The anode is an aluminum wire of 1.5 mm diameter and approximately 15 m long laid out in a spiral pattern 10 cm above the mirror, but fully submerged in the electrolyte.
Quality anodized coatings are very sensitive to the cleanliness of both the glass and evaporated aluminum. During anodization any impurities present create high electrical fields which accelerate the reaction, breaking aluminum surface bonding and causing pinholes. It is important to anodize the mirror immediately after coating as some amount of oxidation occurs naturally in the atmosphere and this oxide will crack as the new layer forms underneath.
The thickness of the anodized layer determines the wavelength at which peak reflectivity of the mirror is obtained. This thickness is controlled by adjusting the voltage across the electrolyte [4]. Typically, 60 V is used at a current of 8 A which oxidizes the top 80 nm of the aluminum coating. This gives a reflectance of 92% at approximately 320 nm (Figure 1). It takes less than 5 minutes to anodize a mirror.
Testing
On-site testing includes measurements of reflectivity, spot size and radius of curvature after coating. Reflectivity is measured using a broad-spectrum light source, an adjustable filter wheel and a photometer (Oriel 71610). All reflectivity measurements are referenced to a calibration mirror of pure aluminum (which is periodically recoated to ensure consistency). Minimum specifications are 90% at 320 nm and ≥ 85% between 280 nm and 450 nm (Figure 2). The reflectivity data is acquired soon after mirror coating to provide a baseline for the determination of mirror quality degradation due to environmental effects.
For spot size and radius of curvature measurements a laser beam is passed through a diffuser to illuminate the entire mirror surface and reflected light is viewed on a screen located 24 m from the mirror. The first measurement is the image size at exactly 24.000 m (the nominal RoC). Next, the absolute minimum spot size is determined by adjusting the target screen distance. The minimum spot size corresponds to the actual radius of curvature and is defined as the smallest circle into which 90% of the reflected light falls (Figures 3 and 4).
Design specifications established a radius of curvature equal to 24 m ± 1% and a spot size <10 mm at RoC. The mirrors had an average RoC of 23.97 ± 0.01 m and an average spot size of 6.0 ± 0.5 mm.
Effects of Exposure on Telescope Mirror Reflectivity
Preliminary reflectivity measurements taken at the beginning of 2007 on the first two telescopes built showed an overall loss of 3% reflectivity per year at 320 nm (Figure 5). See [5] for more information on the weathering of mirrors at the observatory.
As the telescopes are in stow position the majority of the time, uneven weathering of the mirrors occurs. Roughly, the upper third of the mirrors are mounted in an overhang, facing downward. These mirrors are less affected by rain and dirt build up. One mirror in this upper region was measured showing only a 1% loss (@320 nm) during the 2.5 years it had been in use. This mirror may be particularly shielded as it is mounted adjacent to the upper quad arm and therefore may not represent the average degradation of the upper telescope.
More recently we have begun regular testing of four mirrors per telescope (two in the upper region and two in the lower region) which will be repeated every three months. Using the first of these long-term measurements we can show the beginning of a trend of reflectivity loss over time. Given the amount and variability of degradation seen on T1 and the possible corresponding effects that would be seen in the long-term drift of the energy threshold and event rate, we plan on recoating these mirrors during the summer of 2007.
Conclusions
On-site aluminization and anodization of the glass facets provided by D.O.T.I. have produced quality mirrors for all four VERITAS telescopes. All design specifications for optics and reflectivity were met. While any reduction in reflectivity is undesirable, the apparent rate of loss is acceptable and should not adversely affect the quality of data produced by the array. Ongoing studies of the degradation of mirror reflectivity over time will help us to optimize the use of our coating facility as well as understand the environment in which our mirrors reside.
Acknowledgments
VERITAS is supported through grants from the Smithsonian Institution, U.S.D.O.E., N.S.F., P.P.A.R.C. (UK), N.S.E.R.C. (Canada), and S.F.I. (Ireland). The authors gratefully acknowledge the help of Ken Gibbs, Dave Hanna, Ken Ragan, Mark Lang, Jim Gaidos, Teresa Lappin and all the collaborators.
References
[1] T. Lappin, A survival guide to mirror coating and anodization, Tech. rep., Fred Lawrence Whipple Observatory (1992).
[2] W. Kindred, J. T. Williams, D. Clark, In situ aluminization of the MMT 6.5 m primary mirror, Tech. rep., Fred Lawrence Whipple Observatory (2003).
[3] K. Harris, T. Lappin, M. A. Lawrence, P. T. Reynolds, Mirror Coating and Anodization at the Whipple Observatory, in: P. Fleury, G. Vacanti (Eds.), Towards a Major Atmospheric Cerenkov Detector for TeV Astro/particle Physics, 1992, p. 189.
[4] G. Haas, On the preparation of hard oxide films with precisely controlled thickness on evaporated aluminum mirrors, Journal of the Optical Society of America 39 (7) (1949) 532.
[5] H. M. Badran, Mirror cleaning and reflectivity degradation at 1300 and 2300 m above sea level at Mt. Hopkins, Arizona, Nuclear Instruments and Methods in Physics Research A 524 (2004) 162–168.
2nd PDF
Mirror Facets for the VERITAS Telescopes
E. Roache, R. Irvin, J. S. Perkins, K. Harris7, A. Falcone™, J. FinleyH and T. Weekes
“Smithsonian Astrophysical Observatory, ‘EOS Technologies, “Pennsylvania State University, “Purdue University roache@egret.sao.arizona.edu
Abstract
Each of the VERITAS telescopes has 345 glass facets. These were manufactured by D.O.T.I. (Roundrock, Texas), by slumping and grinding to obtain the desired optical figure. The facets were aluminized and anodized at the Whipple Observatory. The reflectivity, radius of curvature and spot size were measured. The design specifications for reflectivity (90% at 320 nm and ≥ 85% between 280 nm and 450 nm), radius of curvature (24 m < ±1%) and spot size (< 10 mm at Radius of Curvature) were easily met. The aluminizing and anodizing process are described as well as the effects of exposure at the VERITAS site on the reflectivity.
Glass
VERITAS mirror facets measure 60.96 ± 0.3 cm across the flat sides (width) with a radius of curvature (RoC) measuring 24 m ± 1%. The mirrors are slumped glass 11.5 ± 1.0 mm thick and aluminized on the front surface.
- The energy concentration of each mirror allows for more than 90% of the reflected light to fall within a 10 mm diameter circle located at the radius of curvature.
- An alignment of all mirrors on the telescope produces a point spread function of 0.06°, which is well within the pixel size of the camera.
To achieve a high quality aluminum coating, it is essential that the glass be thoroughly cleaned. The glass is washed with a phosphate-free mild detergent (Liquinox) to remove the surface dirt. This is followed by a rinsing with tap water and a final rinsing with distilled water. The glass is then dried in an upright position to help keep it clean. Prior to loading the glass into the aluminizing chamber, the glass is wiped with isopropyl alcohol (99% electronic grade). Once in the chamber, the glass is “dusted” with carbon dioxide snow, which removes any lint or dust present on the glass surface. A final microscopic cleaning using ionized argon is performed under vacuum just prior to the deposition of aluminum [4].
Aluminizing
Aluminizing is the process of evaporating aluminum onto the glass surface to create a mirror. The evaporation must be done under vacuum to ensure the purity of the coating, which is important for optical properties and strong adhesion [3].
- The glass is suspended from the top, facing downwards.
- 75 cm below the glass is a 7.5 cm long tungsten filament.
- The filament supports 30–40 aluminum staples consisting of 99.999% pure, 1 mm diameter aluminum cut to a length of approximately 4 cm.
- The final vacuum needed for deposition is in the mid 10⁻⁵ Torr range.
- The thickness of the coating is measured using a 5 MHz quartz crystal oscillator mounted inside the chamber adjacent to the glass facet [2].
- The average aluminum coating is 180 nm thick, deposited at a rate of between 3 and 8 nm per second.
- The entire coating process (per mirror) takes about one hour.
Anodizing
Anodization is a process in which the top layer of the pure aluminum coating is converted into a harder and more durable layer of aluminum oxide. This is accomplished by passing an electrical current through the aluminum coating while it is submerged in an electrolyte solution. Compared to a quartz overcoat, the anodized surface is much less prone to deterioration, is less costly to produce and can be washed as needed.
- The electrical circuit consists of the cathode (mirror surface), electrolyte solution and the anode (aluminum coil).
- The electrolyte is a weak acidic solution (pH 5.5) containing ammonium hydroxide, tartaric acid, distilled water and ethylene glycol.
- The anode is an aluminum wire of 1.5 mm diameter and approximately 15 m long laid out in a spiral pattern 10 cm above the mirror, but fully submerged in the electrolyte [2].
Quality anodized coatings are very sensitive to the cleanliness of both the glass and evaporated aluminum. During anodization any impurities present create high electrical fields which accelerate the reaction, breaking the aluminum surface bonding and causing pinholes. It is important to anodize the mirror immediately after coating as some amount of oxidation occurs naturally in the atmosphere and this oxide will crack as the new layer forms underneath.
The thickness of the anodized layer determines the wavelength at which peak reflectivity of the mirror is obtained. This thickness is controlled by adjusting the voltage across the electrolyte [1]. Typically, 60 V is used at a current of 8 A which oxidizes the top 80 nm of the aluminum coating. This gives a reflectance of 92% at approximately 320 nm. It takes less than 5 minutes to anodize a mirror.
Testing and Validation
On-site testing includes measurements of reflectivity, spot size and radius of curvature after coating.
- Reflectivity is measured using a broad-spectrum light source, an adjustable filter wheel and a photometer (Oriel 71610).
- All reflectivity measurements are referenced to a calibration mirror of pure aluminum (which is periodically recoated to ensure consistency).
For spot size and radius of curvature measurements a laser beam is passed through a diffuser to illuminate the entire mirror surface and reflected light is viewed on a screen located 24 m from the mirror. We measure:
- the image size at 24 m (the nominal RoC)
- by adjusting the target distance, the minimum spot size
The minimum spot size corresponds to the actual RoC and is defined by the smallest circle into which 90% of the reflected light falls.
Design specifications established a RoC equal to 24 m ± 1% and a spot size < 10 mm at RoC. The mirrors had an average RoC of 23.97 ± 0.01 m and an average spot size of 6.0 ± 0.5 mm.
Effects of Exposure on Reflectivity
Preliminary reflectivity measurements taken at the beginning of 2007 on the first two telescopes showed an overall loss of 3% reflectivity per year at 320 nm. More recently we have begun regular testing of four mirrors per telescope (two in the upper region and two in the lower region) which will be repeated every three months. Using the first of these long-term measurements we can show the beginning of a trend of reflectivity loss over time. Given the amount of degradation seen on the first telescope, we plan on recoating those mirrors in the summer of 2007.
Conclusions
On-site aluminization and anodization of the glass facets have produced quality mirrors for all four VERITAS telescopes. All design specifications for optics and reflectivity were met. While any reduction in reflectivity is undesirable, the apparent rate of loss is acceptable and should not adversely affect the quality of data produced by the array. Ongoing studies of the degradation of mirror reflectivity over time will help us to optimize the use of our coating facility as well as understand the environment in which our mirrors reside.
References
[1] G. Haas. On the preparation of hard oxide films with precisely controlled thickness on evaporated aluminum mirrors. Journal of the Optical Society of America, 39(7):532, 1949.
[2] K. Harris, T. Lappin, M. A. Lawrence, and P. T. Reynolds. Mirror Coating and Anodization at the Whipple Observatory. In P. Fleury and G. Vacanti, editors, Towards a Major Atmospheric Cerenkov Detector for TeV Astro/particle Physics, page 189, June 1992.
[3] W. Kindred, J. T. Williams, and D. Clark. In situ aluminization of the MMT 6.5m primary mirror. Technical report, Fred Lawrence Whipple Observatory, 2003.
[4] T. Lappin. A survival guide to mirror coating and anodization. Technical report, Fred Lawrence Whipple Observatory, 1992.
Acknowledgments: VERITAS is supported by grants from the Smithsonian Institution, U.S. DOE, NSF, PPARC (UK), NSERC (Canada), and SFI (Ireland). The authors gratefully acknowledge the help of Ken Gibbs, Dave Hanna, Ken Ragan, Mark Lang, Jim Gaidos, Teresa Lappin and all the collaborators and students who spent time in the mirror lab, outside in the hot AZ sun installing mounting hardware on the telescopes, or working in the middle of the night on alignment. Thank You.
